MU Chemical Engineering (Semester 6)
Mass Transfer Operation - 2
May 2016
Total marks: --
Total time: --
INSTRUCTIONS
(1) Assume appropriate data and state your reasons
(2) Marks are given to the right of every question
(3) Draw neat diagrams wherever necessary


1(a) Define q factor is distillation and give its significance.
4 M
1(b) Discuss the selection criteria for solvent liquid-liquid extraction.
4 M
1(c) Explain the factors affecting leaching operation.
4 M
1(d) Give the properties of adsorbents.
4 M
1(e) State and explain the &Delta
4 M

2 For a binary system of heptane-ethylbenzene the equilibrium data are as follows:
x 0 0.08 0.185 0.251 0.333 0.487 0.651 0.788 0.914 1
y 0 0.233 0.428 0.514 0.618 0.729 0.834 0.904 0.963 1

A feed mixture composed of 42 mole% heptane and 58 mole% ethyl benzene is to be fractionated to yield an overhead product of 197 mole% heptane and a residue of 99 mole ethyl benzene.
(i) Using reflux ratio of 1.5 find the number of equilibrium stages needed for saturated liquid feed and a bubble point reflux by the McCabe-Thiele method.
(ii) Find the minimum reflux ratio.
(iii) Find the number of equilibrium stages at total reflux.
20 M

3(a) Give the procedure to find the height of packed bed for liquid-liquid extraction tower.
10 M
3(b) Derive Fenske's equation for minimum no. Of stages at total reflux.
10 M

4(a) Explain the construction and working of Bollmann extractor.
6 M
4(b) For extraction of dioxane from water, benzene is used as an extraction solvent. At 298K, the equilibrium distribution of dioxane between water and benzene is as given below:
  Weight % dioxane in water   5.1   18.9   25.2
  Weight % dioxane in benzene   5.2   22.5   32

At these concentrations, water and benzene are substantially insouluble 1000kg of solution containing 25% dioxane is to be extracted with benzene to remove 95% of the dioxane free benzene is used.
(i) calculate the solvent requirement for single batch operation.
(ii) If the extraction were done: in four stages cross current unit using 750 kg of pure benzene each time, determine the final raffinate concentration and the percentage removal of dioxane from feed solution.
14 M

5(a) Discuss the adsorption in fixed beds. Explain break through curve and adsorption zone.
10 M
5(b) A hot solution of 5000kg containing Na2CO3 and water with a concentration of 25% by weight Na2CO3 is cooled to 20°
10 M

Write short notes on any Four out of following
6(a) Minimum and maximum boiling azeotropes.
5 M
6(b) Ion Exchange
5 M
6(c) Hollow and spiral wound membranes
5 M
6(d) Reverse osmosis
5 M
6(e) Oslo cooling crystallizer
5 M



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